Effect of Calcination Temperature on The Synthesis of Silica from Bagasse
Poedji Loekitowati Hariani, Fahma Riyanti, Desneli Desneli, Fatma Fatma, Sabila Yunita, Muhammad Said
J. Pure App. Chem. Res. Vol 10, No 2 (2021), pp. 140 - 147
Submitted: March 04, 2021     Accepted: August 31, 2021     Published: August 31, 2021
DOI: http://dx.doi.org/10.21776/ub.jpacr.2021.010.02.587

Abstract


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Bagasse is the solid waste derived from the sugar-making process. A large amount of silica in bagasse is a potential source of silica. In this study, extraction of silica from bagasse was carried out in the following steps: pretreatment of bagasse using HCl solution, followed by calcination at varying temperatures (700℃, 800℃, and 900℃) using a furnace. Furthermore, extraction using NaOH solution and precipitation using HCl. Silica characteristics were obtained using X-Ray Diffraction (XRD), Scanning Electron Microscopy-Electron Dispersive Spectrometry (SEM-EDS), and BET surface area. The results showed that calcination temperature affected the characteristics of the silica produced. The silica extracted at 700℃ produced an amorphous phase with a broad peak at an angle of 2θ = 20-24°. It contained the most considerable silica content and surface area, 42.46% and 796.89 cm2/g, respectively. The extracted silica had an average diameter of 5.67 mm and a pore volume of 1.184 cm3/g.


Keywords : silica, bagasse, calcination temperature
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