Identification of volatile compounds in several meat and bone broth using Solid Phase Micro Extraction-Gas Chromatography Mass Spectrometry (SPME-GCMS) for initial detection of Halal and Non-Halal Food
Diana Candra Dewi, Chanif Mahdi, Hermin Sulistyarti, Aulani`am Aulani`am
J. Pure App. Chem. Res. Vol 12, No 2 (2023), pp. 65-79
Submitted: April 15, 2023     Accepted: June 23, 2023     Published: August 28, 2023
DOI: http://dx.doi.org/10.21776/ub.jpacr.2023.012.02.3308

Abstract


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The development of techniques for detecting halal and non-halal animal meat is of great importance as a useful tool for monitoring and assuring food quality for Muslim. Flavor or aroma is one of the sensory attributes for consumers to distinguish broth cattle. The differences aroma of broth cattle is contributed by the content of volatile compounds. This study was aimed to determine the composition of volatile compounds in meat and bone broth from five different animals, i.e., cow (beef), pig (pork), goat, lamb, and chicken for initial identification of halal and non halal food. A preliminary test for samples of meat and bone broth was done by identifying their physical properties including pH, viscosity, and density. The volatile compounds in meat and broth samples were extracted using a solid phase-micro extraction (SPME) at room temperature and analyzed by gas chromatography-mass spectrometry (GCMS). The results revealed the physical properties of meat and bone broth, i.e. pH, viscosity, and density, cannot be used to distinguish the type of broth produced from beef, pork, goat, lamb, and chicken. Successful results for the identification were achieved through chromatogram profile of volatile compounds from meat and bone broth which show characteristics to each type of animal, and therefore it can be used to distinguish pork from beef, goat, lamb, and chicken as initial detection for halal and non halal food. The research also identified 7 predominant volatile compounds as a marker for meat pork and other 8 specific compounds marker for pork bone.


Keywords : Halal; meat; bone; broth; volatile
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References


[1] Windarsih, A., Riswanto, F.D.O., Abu Bakar, N.K., Yuliana, N.D., Dachriyanus and Rohman, A., Molecules, 2022, 27, 8325, 1-14

[2] Resconi, V. C., Escudero, A., and Campo M. M., Molecules, 2013, 18, 6748-6781

[3] Miller, R., Foods, 2020, 9, 428, 1-25

[4] Perestam, A.T., Fujisaki, K.K., Nava, O., and Hellberg, R.S., Food Control, 2017, 71, 346–352

[5] Jiang, X., Rao, Q., Mittl, K., and Hsieh, Y.H.P., Food Control, 2020, 110, 107045, 1-8

[6] Wang, Yao., Song, Huanlu., Zhang, Yu., Tang, Jiani., Yu, Donghai., Flavour Fragr. J., 2016, 31, 319-328

[7] Zhang, M., Karangwa, E., Duhoranimana, E., Zhang, X., Xia, S., Yu, J., and Xu, M., 2017, Flavour Fragr. J. 2017;1–14

[8] Zhao, Jian., Wang, Meng., Xie, Jianchun., Zhao, Mengyao., Hou, Li., Liang, Jingjing., Wang, Shi., Cheng., Jie.,. Food Chemistry, 2017, 226, 51-60

[9] Sun Yanwen., Fu Mangjuan., Li Zhicheng., Peng Xiaoli., Food Analytical Methods, 2018, 11, 1321–1329

[10] Belitz, H.D., Grosch, W., Schieberle, P., Food Chemistry, 4th revised and extended ed, 2009, Springer, Verlag Berlin Heidelberg, 606

[11] Wang, X., Zhu, L., Han, Y., Xu, L., Jin, J., Cai, Y. dan Wang, H. Journal of Food Processing and Preservation, 2017, 13503, 1-8

[12] Machiels, D., van Ruth, S.M., Posthumus., M.A., and Istasse, L., 2003, Talanta, 2003, 60 755-764

[13] Choudhury, B. H., Volatile and Non-Volatile Components of Beef Marrow Bone Stock. Dissertasion. 2008, State University of New Jersey, USA

[14] Priolo, A., Cornu, S., Prache, S., Krogmann,M., Kondjoyan,N., Micol, D., and Berdague, J.L, Meat Science, 2004, 66, 475–481

[15] Qi, Shasha., Wang, Peng., Zhan, Ping., Tian, Honglei., Food Chemistry, 2022, 371 131111

[16] Krvavica, M., Bradaš, M., Rogošić, J., Jug, T., Vnučec, I., Radovčić, M.N., MESO, First Croation Journal on Meat, 2015, No. 3, Vol. XVII, 264-271

[17] Kabagias, I.K., Foods, 2018, 7, 40, 1-11

[18] Gąsior Robert., Kawęcka Aldona., Wojtycza Krzysztof., Sikora Jacek., Ann. Anim. Sci., 2021, Vol. 21, No. 1, 331–346

[19] Gkaranea Vasiliki, Bruntona Nigel P., Allenb Paul, Gravadora Rufielyn S., Claffeyc Noel A., Diskinc Michael G., Faheya Alan G., Farmerd Linda J., Moloneye Aidan P., Alcaldef Maria J., Murphyg Patrick, Monahana Frank J., Food Research International 2019, 115, 54–64

[20] Madruga, M.S., Stephen Elmore, J., Oruna-Concha, M.J., Balagiannis, D., and Mottram, D.S, Food Chemistry, 2010, 123, 513–520

[21] Feng Yunzi, Cai Yu, Fu Xiong, Zheng Lin, Xiao Zuobing, Zhao Mouming, Food Chemistry, 2018, 265, 274-280

[22] Geng, Q., Zhan, P., Tian, H., Wang., P., and Chen, H., Hindawi International Journal of Analytical Chemistry 2019, 1-11

[23] Bueno, M., Resconi, V.C., Campo, M.M, Ferreira, V., and Escudero, A., Food Chemistry, 2018, 281, 49-56

[24] Spietelun, A., Kloskowski, A., Chrzanowski, W., and Namiesnik, J., Chemical Review, ACS, 2013, 113, 1667−1685

[25] Brunton, N.P., Cronin, D.A., Monahan, F.J., and Durcan, R., Food Chemistry, 2000, 68 339-345

[26] Kataoka, Hiroyuki., Lord, Heather L., Pawliszyn, Janusz., Journal of Chromatography A 2000, 880, 35-62


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